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18 Hydrolysis of regular viscose in 4 M HCl at 100°C. Extrapolation of curves gives the amorphous (ao) and crystalline (co) fractions in the untreated fibre. ) Contents Home 24 CELLULOSE: STRUCTURE, PROPERTIES AND BEHAVIOUR IN THE DYEING PROCESS each anhydroglucose unit were determined and conclusions were drawn about the structure of the elementary fibrils. Rowland and coworkers [34,109] did similar experiments with N,N-diethylaziridium chloride (DAC), which introduces N,Ndiethylaminoethyl groups, (C2H5)2N–CH2CH2–, into the cellulose, and have suggested that these methods may well provide an insight into the supramolecular structure of cellulose that is not forthcoming from physical measurements.

The difference between refractive indices for light polarised parallel and perpendicular to the fibre axis. r. spectroscopy [112] has also been used to measure the orientation factor. The method depends on the absorption of radiation by a particular chemical group in the chain molecule. r. radiation and only the component of the oscillations parallel to the electric vector is effective. e. at right angles to the plane of polarisation) and absorption should be zero perpendicular to the electric vector.

The effect of the introduction of hemiacetal crosslinks into paper is an immediate increase in wet strength because in this case the crosslinks are predominantly between the fibres [171,172]. g. dyeing and finishing, paper making. (2) Cellulose cannot easily be freed from water completely; the fibres normally contain adsorbed water in quantities determined by the relative humidity and temperature of the surrounding atmosphere. (3) The mechanical properties of cellulosic fibres vary with their moisture content.

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