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By O. I. Milner

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N . and O ' H A R A , F. , Anal. Chem. 2 9 , 1318-22 (1957). 62. H O U G H T O N , Ν . , Anal. Chem. 2 9 , 1513-5 (1957). 63. C A L I , L . J . , LOVELAND, J. , and PARTIKIAN, D . G . , Anal. Chem. 3 0 , 7 4 - 7 (1958). 64. ALBERT, D . K. , Anal. 31,1593-6 (1959). 65. , Chimie Analytique 4 0 , 120-6 (1958). 66. B R O W N , C. , Anal. Chem. 3 2 , 4 4 2 - 3 (1960). 67. FARLEY, L. , DETERT, F. , Anal. Chem. 3 2 , 142-3 (1960). N I C K S I C , S. , and W E B B , W. , 68. Am. Soc. Testing Materials, Method D l 29-58 ; Institute of Petroleum, Method IP 61/53.

The less sensitive molybdenumblue color method has also been used [6, 9] ; in the version employed in the author's laboratory, adequate sensitivity was achieved by use of a specially designed spectrophotometer cell. Emission spectroscopy [10] and neutron activation [6] have also been used to determine the arsenic collected on a solid adsorbent. The former method has relatively poor precision, whereas the latter is too specialized for general use. In the most recent work, the color reaction between arsine and silver diethyldithiocarbamate in pyridine [11] has been used to estimate the arsenic.

L Y N C H , G . , Analyst 7 9 , 137 (1954). 36. M I D D L E T O N , G . , and STUCKEY, R. , Analyst 7 8 , 532-42 (1953). 37. Society for Analytical Chemistry, Report of Sub-committee on Metallic Impurities in Organic Matter, Analyst 8 5 , 643 (1960). 38. National Safety Council Data Sheet D-311 ( D - C h e m 44) on Perchloric Acid. 39. S M I T H , G . F . , Anal. Chim. Acta 8 , 397-421 (1953). 40. , L'Action de Γ Acide Perchlorique sur Les Matières Organique, Hermann et Cie, Paris. (1934). 41. FORRESTER, J.

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