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By Dan P. Manka

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1% or better are claimed by one pump manufacturer. The major limitation of the pump method is that the gases come into contact with the pump oil. Therefore, it is limited to use with light gases, such as hydrogen, air, or carbon dioxide, that do not react with the pump materials and are not dissolved in the oil. 2. MOTOR-DRIVEN SYRINGES Motor-driven syringes are available that can meter one or more gases into a flowing gas stream (Nelson and Taylor, 1971). This method may be suitable for short-term experiments where maximum precision is not required.

1972). By this method a sample containing nitric oxide is partially reacted with ozone, and the reduction in the concentration of nitric oxide is measured with a suitable analyzer (such as a chemiluminescent analyzer). Assuming that the reduction in the nitric oxide concentration results from the formation of nitrogen dioxide, the change in nitric oxide concentration is the same as the nitrogen dioxide produced. The ozone used for the titration is generated by an ultraviolet lamp as described in Section III,C,9,a.

An automatic shutoff valve, programmed to open a few seconds before the sample inject valve is actuated, is installed downstream of the sample inject valve. 5-1 ml of fresh liquid to flow rapidly through the sample inject valve, fill the sample port, and flush out any gas bubbles that might have accumulated since the last sample injection. This method permits conditions to be optimized so that premature vaporization of the mixture is avoided while consumption of the standard is minimized. Also, it permits sealing off the standard so it will not evaporate.

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